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1、Designation:E1004?09StardTestMethodfDeterminingElectricalConductivityUsingtheElectromagic(EddyCurrent)Method1ThisstardisissuedunderthefixeddesignationE1004thenumberimmediatelyfollowingthedesignationindicatestheyearofigin
2、aladoptioninthecaseofrevisiontheyearoflastrevision.Anumberinparenthesesindicatestheyearoflastreapproval.Asuperepsilon()indicatesaneditialchangesincethelastrevisionreapproval.ThisstardhasbeenapprovedfusebyagenciesoftheDep
3、artmentofDefense.1.Scope1.1Thistestmethodcoversaprocedurefdeterminingtheelectricalconductivityofnonmagicmetalsusingtheelectromagic(eddycurrent)method.Theprocedurehasbeenwrittenprimarilyfusewithcommerciallyavailabledirect
4、readingelectricalconductivityinstruments.Generalpurposeeddycurrentinstrumentsmayalsobeusedfelectricalconductivitymeasurementsbutwillnotbeaddressedinthistestmethod.1.2Thistestmethodisapplicabletometalsthathaveeitheraflats
5、lightlycurvedsurfaceincludesmetalswithwithoutathinnonconductivecoating.1.3Eddycurrentdeterminationsofelectricalconductivitymaybeusedinthestingofmetalswithrespecttovariablessuchastypeofalloyagingcolddefmationheattreatment
6、effectsassociatedwithnonunifmheatingoverheatingeffectsofcrosion.Theusefulnessoftheexaminationsofthesepropertiesisdependentontheamountofelectricalconductivitychangecausedbyachangeinthespecificvariable.1.4Electricalconduct
7、ivitywhenevaluatedwitheddycurrentinstrumentsisusuallyexpressedasapercentageoftheconductivityoftheInternationalAnnealedCopperStard(IACS).TheconductivityoftheAnnealedCopperStardisdefinedtobe0.58108Sm(100%IACS)at20C.1.5Thev
8、aluesstatedinSIunitsareregardedasstard.1.6Thisstarddoesnotpurpttoaddressallofthesafetyconcernsifanyassociatedwithitsuse.Itistheresponsibilityoftheuserofthisstardtoestablishappropriatesafetyhealthpracticesdeterminetheappl
9、icabilityofregulatylimitationspritouse.2.ReferencedDocuments2.1ASTMStards:2B193TestMethodfResistivityofElectricalConductMaterialsE105PracticefProbabilitySamplingofMaterialsE122PracticefCalculatingSampleSizetoEstimateWith
10、SpecifiedPrecisiontheAveragefaacteristicofaLotProcessE543SpecificationfAgenciesPerfmingNondestructiveTestingE1316TerminologyfNondestructiveExaminations2.2ASNTDocuments:RecommendedPracticeSNTTC1AfPersonnelQualificationCer
11、tificationInNondestructiveTesting3ANSIASNTCP189StardfQualificationCertificationofNDTPersonnel32.3AIADocument:NAS–410CertificationQualificationofNondestructiveTestingPersonnel43.Terminology3.1Definitions—Definitionsofterm
12、srelatingtoeddycurrentexaminationaregiveninTerminologyE1316.3.2DefinitionsofTermsSpecifictoThisStard:3.2.1temperaturecoeff?cient—thefractionalpercentagechangeinelectricalconductivityperdegreeCelsiuschangeintemperature.4.
13、SignificanceUse4.1Absoluteprobecoilmethodswhenusedinconjunctionwithreferencestardsofknownvalueprovideameansfdeterminingtheelectricalconductivityofnonmagicmaterials.1ThistestmethodisunderthejurisdictionofASTMCommitteeE07o
14、nNondestructiveTestingisthedirectresponsibilityofSubcommitteeE07.07onElectromagicMethod.CurrenteditionapprovedMay152009.PublishedJune2009.iginallyapprovedin1991.Lastpreviouseditionapprovedin2002asE100402.DOI:10.1520E1004
15、09.2FreferencedASTMstardsvisittheASTMwebsitewww.astm.gcontactASTMCustomerServiceat.FAnnualBookofASTMStardsvolumeinfmationrefertothestard’sDocumentSummarypageontheASTMwebsite.3AvailablefromAmericanSocietyfNondestructiveTe
16、sting(ASNT)P.O.Box285181711ArlingateLn.ColumbusOH432280518:www.asnt.g.4AvailablefromAerospaceIndustriesAssociationofAmericaInc.(AIA)1000WilsonBlvd.Suite1700ArlingtonVA222093928:www.aiaaerospace.g.ASummaryofChangessection
17、appearsattheendofthisstardCopyright?ASTMInternational100BarrHarbDrivePOBoxC700WestConshohockenPA194282959.UnitedStates1d5K=~1r!fr~cm!K.50r51(2)d51=psf~m!5o54p31027r51(3)where:s=electricalconductivityofthesampleinSmr=elec
18、tricalresistivityinVmf=examinationfrequencyinHz.Thesefmulasarefnonmagicmaterialswhentherelativepermeabilityrel=1.Ifthethicknessofthesamplethereferencestardsisatleast2.6dtheeffectofthicknessisnegligible.Smallerdepthsofper
19、ation(higherfrequencies)maybedesirablefmeasuringsurfaceeffects.Theeddycurrentdensitydecreasewithdepthisalsoaffectedbythecoildiameter.Thechangeduetocoildiametervariationisnotconsideredintheaboveequation.Consulttheinstrume
20、ntmanufacturerifperationdepthappearstobeasourceoferrinthemeasurement.8.Apparatus8.1ElectronicApparatus—Theelectronicapparatusshallbecapableofenergizingtheprobecoilwithalternatingcurrentsofsuitablefrequenciespowerlevelssh
21、allbecapableofsensingchangesinthemeasuredimpedanceofthecoil.Equipmentmayincludeanysuitablesignalprocessingdevice(phasediscriminatfiltercircuitssofth).Theoutputmaybedisplayedineitheranalogdigitalreadouts.Readoutisnmallyin
22、percentIACSalthoughitmaybescaledfreadingsinotherunits.Additionalapparatussuchascomputersplottersprinterscombinationthereofmaybeusedintherecdingofdata.8.2Probe—Probecoildesignscombineempiricalmathematicaldesignmethodstoch
23、ooseappropriatecombinationsofacteristics.Manyinstrumentsuseoneprobecoil.Ininstrumentswithseveralcoilsthedifferencebetweencoilsisthecoilgeometry.Fmostconductivityinstrumentsthecableconnectingthecoiltotheinstrumentisaninte
24、gralpartofthemeasuringcircuitthecablelengthshouldnotbemodifiedwithoutconsultingtheinstrumentmanufacturermanual.8.2.1Theprobecoilshouldbedesignedtominimizetheeffectofheattransferfromhtocoil.8.3Mechanicalhlingapparatusffee
25、dingthesamplesmovingtheprobecoilbothmaybeusedtoautomateaspecificmeasurement.9.StardizationCalibration9.1Stardization—Turntheinstrumentonallowitsufficienttimetostabilizeinaccdancewiththemanufacturer’sinstructions.Adjustba
26、lancestardizetheconductivitymeteragainsttheinstrument’soperationalstardscompensatetheconductivitymeterfsurfaceroughnessliftoffinaccdancewiththemanufacturer’sinstructions.Ifaliftoffadjustmentisnotavailabledeterminetheacce
27、ptablerangeofliftoffthatwillmeettheaccuracyrequirements.Verifythestardizationoftheconductivitymeteratperiodicintervals(seeSection10).9.1.1Theinstrumentprobereferencestardsshallbestardizedwhilemaintainingthetemperaturewit
28、hin5Foftheambienttemperature.Itisdesirabletoperfmthestardizationatroomtemperature(typically70615F).9.1.2Instrumentswithtwostardizationadjustmentsshallbeadjustedsothattheknownvalueofconductivityisobtainedfbothreferencesta
29、rds.Thereferencestardsusedshouldhaveconductivitiesthatbrackettheconductivityvalueofthesample.9.1.3Someinstrumentshaveonlyonestardizationadjustment.Inthesecasestheinstrumentshouldbestardizedtoareferencestardatoneendofther
30、angetobeexamined.Areferencestardattheotherendoftherangeshouldbeexaminedtoverifythattheerriswithinacceptablelimitsovertheentirerange.9.2ReferenceStards—Electricalconductivityreferencestardsareusuallyclassifiedasprimarysec
31、ondaryoperationalstards.9.2.1PrimaryConductivityStards—Thesearereferencestardsthathavebeenverifiedintermsofthefundamentalunits.Theprimarystardsarekeptinalabatyenvironmentareusedonlytostardizesecondarystards.9.2.2Secondar
32、yConductivityStards—Thesereferencestardshaveavalueassignedthroughcomparisonwithprimarystards.TheprimarystardsusedfassignmentofvaluestothesesecondarystardsshallhavebeenstandardizedusingTestMethodB193.Thesecondarystardsare
33、keptinalabatyenvironmentareusedonlytocalibrateoperationalinstrumentstards.9.2.3OperationalConductivityStards—Thesereferencestardsarestardizedbycomparisonwithsecondarystards.Thesereferencestardsareusedtostardizetheinstrum
34、entduringuse.9.3Referencestardsshouldbeexaminedwitharelativelysmallcoiltodeterminetheunifmityofelectricalconductivityoverthesurfaceofthestard.Boththefrontthebacksurfaceshouldbeexaminedfanyconductivitydifferencesthatmayex
35、ist.Ifpossiblescanthesurfacesatseveraldifferentinputsignalfrequencies.9.4Eachtimethereferencestardsareusedplacetheprobecoilatthesamepositionrelativetothecenterofthestardwithin61?2ofthecoildiameternottoexceed66.35mm(60.25
36、in.)fexample:64mmfan8mmdiametercoil62mmfa4mmdiametercoil.9.5Electricalconductivityreferencestardsarepreciseelectricalstardsshouldbetreatedassuch.Scratchingofthesurfaceofthestardmayintroducemeasurementerr.Avoidpingotherro
37、ughhlingofthestard.Keepthesurfaceofthestardascleanaspossible.Cleanwithanonreactiveliquidasoftclothtissue.Stereferencestardsinaplacewherethetemperatureisrelativelyconstant.Avoidthermalshockingofthereferencestardsplacingth
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